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Beilstein J. Org. Chem. 2009, 5, No. 6, doi:10.3762/bjoc.5.6
Graphical Abstract
Figure 1: Donors and acceptor compounds.
Scheme 1: Synthesis of π-extended dithiafulvalenes 7a and 7b. i) n-BuLi/THF, −78 °C, 15 min, then rt, overnig...
Scheme 2: Synthesis of π-extended dithiafulvalenes 8 and 9. i) 6, n-BuLi, THF, −78 °C, 15 min; then, 5c, −78 ...
Scheme 3: Synthesis of π-extended dithiafulvalenes 10. i) 6, n-BuLi, THF, −78 °C, 15 min; then 5d, −20 to 0 °...
Scheme 4: Synthesis of π-extended dithiafulvalenes 11 and dithiafulvalene 12. i) 6, n-BuLi, THF, −78 °C, 15 m...
Figure 2: Cyclic voltammetry (CV) of compounds 8, 10 and 11 in CH2Cl2 at scan rate 100 mV.